(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran

Base Information

• Chemical Name: (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran
• CAS No.: 118270-88-5
• Molecular Formula: C₅₅H₆₂O₇
• Molecular Weight: 835.093

Synonyms:(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran

Chemical Property of (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran

Chemical Property:

Purity/Quality:

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Technology Process of (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran

There total 3 articles about (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mono-4-methoxytrityl chloride (14470-28-1) → (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran (118270-88-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 24 h

2: NaH (60percent, dispersion in oil) / dimethylformamide / 16 h / Ambient temperature

With sodium hydride; In pyridine; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(88)84115-6

Reference yield:

n-octyl β-D-glucopyranoside (29836-26-8) → (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran (118270-88-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 24 h

2: NaH (60percent, dispersion in oil) / dimethylformamide / 16 h / Ambient temperature

With sodium hydride; In pyridine; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(88)84115-6

Reference yield:

benzyl bromide (100-39-0) + (2R,3S,4S,5R,6R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran-3,4,5-triol (118249-71-1) → (2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran (118270-88-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

DOI:10.1016/0008-6215(88)84115-6

upstream raw materials:

benzyl bromide

(2R,3S,4S,5R,6R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-6-octyloxy-tetrahydro-pyran-3,4,5-triol

mono-4-methoxytrityl chloride

n-octyl β-D-glucopyranoside

Downstream raw materials:

octyl 6-O-(2-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

(2S,3S,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-octyloxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-3-ol

octyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

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