methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester
CAS No.:1026544-31-9
Molecular Formula:C₂₄H₃₉N₃O₃
Molecular Weight:417.592
Hs Code.:

methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid <i>tert</i>-butyl ester

Synonyms:methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

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Chemical Property of methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

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Technology Process of methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

There total 1 articles about methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36768-62-4
4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE

: 37553-65-4,64263-83-8,85466-66-6
N-tert-butoxycarbonyl-N-methyl-D-phenylalanine

: 1026544-31-9
methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: N-tert-butoxycarbonyl-N-methyl-D-phenylalanine; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE; With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 72h;
DOI:10.1016/S0223-5234(02)01370-3

Reference yield:

: 1026544-31-9
methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

: 2-methylamino-3-phenyl-N-(2,2,6,6-tetramethyl-piperidin-4-yl)-propionamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/S0223-5234(02)01370-3

Reference yield:

: 1026544-31-9
methyl-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

: 1026341-92-3
N-methyl-2-methylamino-3-naphthalen-2-yl-N-[2-phenyl-1-(2,2,6,6-tetramethyl-piperidin-4-ylcarbamoyl)-ethyl]-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

2.1: HOAt; EDAC*HCl / CH₂Cl₂; dimethylformamide / 0.33 h / 0 °C

2.2: iPr₂NEt / CH₂Cl₂; dimethylformamide / 72 h / 0 - 20 °C

3.1: trifluoroacetic acid / CH₂Cl₂ / 0.83 h / 0 °C

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0223-5234(02)01370-3