Technology Process of C25H18O
There total 3 articles about C25H18O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; caesium carbonate; triphenylphosphine;
In
N,N-dimethyl acetamide;
at 140 ℃;
for 14h;
Inert atmosphere;
DOI:10.1021/ol400738r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: indium(III) triflate / toluene / 0.67 h / 120 °C / 1551.49 Torr / Microwave irradiation
2: caesium carbonate; triphenylphosphine; palladium diacetate / N,N-dimethyl acetamide / 14 h / 140 °C / Inert atmosphere
With
indium(III) triflate; palladium diacetate; caesium carbonate; triphenylphosphine;
In
N,N-dimethyl acetamide; toluene;
2: |Heck Reaction;
DOI:10.1021/ol400738r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: indium(III) triflate / toluene / 0.67 h / 120 °C / 1551.49 Torr / Microwave irradiation
2: caesium carbonate; triphenylphosphine; palladium diacetate / N,N-dimethyl acetamide / 14 h / 140 °C / Inert atmosphere
With
indium(III) triflate; palladium diacetate; caesium carbonate; triphenylphosphine;
In
N,N-dimethyl acetamide; toluene;
2: |Heck Reaction;
DOI:10.1021/ol400738r