8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

Base Information

Chemical Name:8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid
CAS No.:1082051-61-3
Molecular Formula:C₂₅H₂₉N₃O₄
Molecular Weight:435.523
Hs Code.:

Synonyms:8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

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Chemical Property of 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

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Technology Process of 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

There total 1 articles about 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1082051-60-2
ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate

: 1082051-61-3
8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2008.07.119

Reference yield: 20.0%

: 1082051-61-3
8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

: 1082051-44-2
N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide

Guidance literature:: With O-(tert-butyldimethylsilanyl)hydroxylamine; benzotriazol-1-yloxy-tris(dimethylamino)-phosphonium chloride; triethylamine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1016/j.bmcl.2008.07.119