ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate

Base Information

• Chemical Name: ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate
• CAS No.: 1082051-60-2
• Molecular Formula: C₂₇H₃₃N₃O₄
• Molecular Weight: 463.577

Synonyms:ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate

Chemical Property of ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate

Chemical Property:

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Technology Process of ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate

There total 1 articles about ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

Ethyl hydrogen suberate (14113-01-0) + 7-amino-1,3-dimethyl-5-phenyl-1H-benzo[e][1,4]diazepin-2(3H)-one (1082051-84-0) → ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate (1082051-60-2)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In chloroform; at 20 ℃; for 72h;

DOI:10.1016/j.bmcl.2008.07.119

Reference yield: 60.0%

ethyl 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoate (1082051-60-2) → 8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid (1082051-61-3)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2008.07.119

upstream raw materials:

Ethyl hydrogen suberate

7-amino-1,3-dimethyl-5-phenyl-1H-benzo[e][1,4]diazepin-2(3H)-one

Downstream raw materials:

8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

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