Na⁽¹⁺⁾Fe(C₆H₅CNON₂C₆H₅)3^(1-)H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

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Chemical Name:Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O
CAS No.:70224-24-7
Molecular Formula:C₃₉H₃₀FeN₉O₃*H₂O*Na
Molecular Weight:769.578
Hs Code.:

Na<sup>(1+)</sup>*Fe(C<sub>6</sub>H<sub>5</sub>CNON<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3<sup>(1-)</sup>*H<sub>2</sub>O=NaFe(C<sub>6</sub>H<sub>5</sub>CNON<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3*H<sub>2</sub>O

Synonyms:Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

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Chemical Property of Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

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Technology Process of Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

There total 1 articles about Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 94978-78-6
bis[tris((phenylazo)benzaldoximato)iron(II)]iron(III) perchlorate

: 70224-24-7
Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

Guidance literature:: With NaOH; In water; acetone; byproducts: Fe(OH)3; aq. NaOH added dropwise to an acetone soln. of the Fe complex under N2;mixt. warmed and stirred for 15 min; a brown ppt. of Fe(OH)3 is deposited, the green soln. filtered, concd.; crystals purified by recrystallization from acetone containing a small amt. of aq. NaOH;

Reference yield: 80.0%

: iron perchlorate hexahydrate

: 70224-24-7
Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

: 94978-78-6
bis[tris((phenylazo)benzaldoximato)iron(II)]iron(III) perchlorate

Guidance literature:: In ethanol; Fe perchlorate added to a soln. of the Fe complex under N2, heating under reflux for 2 h, black solid filtered off, washed with water, dried invacuo over P4O10;

Reference yield: 55.0%

: 70224-24-7
Na⁽¹⁺⁾*Fe(C₆H₅CNON₂C₆H₅)3^(1-)*H₂O=NaFe(C₆H₅CNON₂C₆H₅)3*H₂O

: 7705-08-0
iron(III) chloride

: 94978-82-2
bis[tris((phenylazo)benzaldoximato)iron(II)]iron(III) tetrachloroferrate

Guidance literature:: In ethanol; anhydrous FeCl3 in EtOH added to a soln. of the Fe complex under N2; mixt. heated under reflux for 2 h; black solid filtered off, washed with water, dried in vacuo over P4O10;