1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

Base Information

Chemical Name:1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone
CAS No.:192379-39-8
Molecular Formula:C₂₁H₁₉N₅O₅
Molecular Weight:421.412
Hs Code.:

1-benzyl-4-nitroimidazole-5-glyoxal (N<sup>2</sup>-benzyl-N<sup>2</sup>-methoxycarbonyl)hydrazone

Synonyms:1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

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Chemical Property of 1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

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Technology Process of 1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

There total 6 articles about 1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 100-39-0
benzyl bromide

: 168412-09-7
1-benzyl-4-nitroimidazole-5-glyoxal (N²-methoxycarbonyl)hydrazone

: 192379-39-8
1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(02)01252-8

Reference yield: 18.0%

: 100-39-0
benzyl bromide

: 168412-08-6
1-benzyl-4-nitroimidazole-5-acetaldehyde (N²-carbomethoxy)hydrazone

: 192379-39-8
1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

Guidance literature:: With oxygen; sodium hydride; In tetrahydrofuran; at 20 ℃; for 10h;
DOI:10.1016/S0040-4020(02)01252-8

Reference yield:

: 99686-99-4
1-benzyl-5-methyl-4-nitro-1H-imidazole

: 192379-39-8
1-benzyl-4-nitroimidazole-5-glyoxal (N²-benzyl-N²-methoxycarbonyl)hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / trifluoroacetic acid / dimethylformamide / Heating

2: 95 percent / acetonitrile / 120 h / Heating

3: 18 percent / NaH; O₂ / tetrahydrofuran / 10 h / 20 °C

With oxygen; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(02)01252-8