N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Base Information

Chemical Name:N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide
CAS No.:696605-56-8
Molecular Formula:C₃₀H₂₈N₂O₂S₂
Molecular Weight:512.697
Hs Code.:

Synonyms:N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

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Chemical Property of N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

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Technology Process of N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

There total 5 articles about N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2987-53-3
2-(Methylthio)aniline

: 91425-33-1
N-hydroxysuccinimidyl 2-[(triphenylmethylthio)methylcarbonylamino]ethanoate

: 696605-56-8
N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: With dmap; In acetonitrile; at 60 ℃; for 6h;
DOI:10.1039/b313996d

Reference yield:

: 34914-36-8
2-(triphenylmethylthio)ethanoic acid

: 696605-56-8
N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / EDCI / acetonitrile / 4 h / 20 °C

2: 98 percent / Et₃N / tetrahydrofuran; dimethylformamide / 3 h / 20 °C

3: 100 percent / NaOH / methanol / 2 h / 40 °C

4: 83 percent / dicyclohexylcarbodimide / tetrahydrofuran / 4 h / 20 °C

5: 60 percent / DMAP / acetonitrile / 6 h / 60 °C

With dmap; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b313996d

Reference yield:

: 91425-31-9
2-(triphenylmethylthio)ethanoic acid-N-hydroxysuccinimido ester

: 696605-56-8
N-(2-thiomethoxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / Et₃N / tetrahydrofuran; dimethylformamide / 3 h / 20 °C

2: 100 percent / NaOH / methanol / 2 h / 40 °C

3: 83 percent / dicyclohexylcarbodimide / tetrahydrofuran / 4 h / 20 °C

4: 60 percent / DMAP / acetonitrile / 6 h / 60 °C

With dmap; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b313996d