3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde

Base Information

• Chemical Name: 3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde
• CAS No.: 178610-55-4
• Molecular Formula: C₂₁H₂₁NO₄
• Molecular Weight: 351.402

Synonyms:3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde

Chemical Property of 3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde

Chemical Property:

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Technology Process of 3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde

There total 2 articles about 3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-[2-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]ethyl]-1,3-dioxolane → 3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde (178610-55-4)

Guidance literature:

With potassium carbonate; acetic acid;

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + (E)-3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)cinnamaldehyde (178238-82-9) → 3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde (178610-55-4)

Guidance literature:

palladium-carbon;

Reference yield: 75.0%

3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propionaldehyde (178610-55-4) + 2-?5-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)[phenyl]-3-pentenyl]-1,3-dioxolan + 2-(1,3-dioxolan-2-yl)ethyl(triphenyl)phosphonium bromide (86608-70-0) → 2-[5-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]pentyl]-1,3-dioxolan

Guidance literature:

With n-butyllithium; palladium-carbon; In tetrahydrofuran; methanol (50 ml)-tetrahydrofuran (THF); nitrogen;

upstream raw materials:

tetrahydrofuran

(E)-3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)cinnamaldehyde

Downstream raw materials:

5-[4-(4-hydroxy-3-methoxyphenyl)butyl]-2,4-oxazolidinedione

ethyl 3-(3-ethoxy-4-hydroxyphenyl)propanoate

ethyl 3-[4-[2-(2-furyl)-5-methyl-4-oxazolylmethoxy]-3-methoxyphenyl]propionate

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