Dimethyl Aminomalonate

Base Information

Chemical Name:Dimethyl Aminomalonate
CAS No.:68641-19-0
Molecular Formula:C₁₈H₁₉NO₅
Molecular Weight:329.353
Hs Code.:

Dimethyl Amino<p-(benzyloxy)phenyl>malonate

Synonyms:Dimethyl Aminomalonate

Suppliers and Price of Dimethyl Aminomalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl Aminomalonate

Chemical Property:

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Technology Process of Dimethyl Aminomalonate

There total 5 articles about Dimethyl Aminomalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: Dimethyl Aminomalonate Hydrochloride

: 68641-19-0
Dimethyl Aminomalonate

Guidance literature:: With sodium hydrogencarbonate; In water;
DOI:10.1021/jo00328a002

Reference yield: 53.0%

: 68641-18-9
Dimethyl Azidomalonate

: 68641-19-0
Dimethyl Aminomalonate

Guidance literature:: With aluminium amalgam; In tetrahydrofuran; diethyl ether; water; at 0 ℃; for 2.5h;
DOI:10.1021/jo00328a002

Reference yield:

: 68641-16-7
(4-benzyloxy-phenyl)-acetic acid methyl ester

: 68641-19-0
Dimethyl Aminomalonate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaH / diethyl ether; methanol / 24 h / Ambient temperature

2: 1.) NaH, HMPA, 2.) p-Toluenesulfonyl azide / 1.) THF, room temp., 2h, 2.) reflux, 2h

3: 53 percent / aluminum amalgam / diethyl ether; tetrahydrofuran; H₂O / 2.5 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; 4-toluenesulfonyl azide; aluminium amalgam; sodium hydride; In tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1021/jo00328a002