N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

Base Information

Chemical Name:N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine
CAS No.:1300749-25-0
Molecular Formula:C₂₁H₂₄N₄O₂S
Molecular Weight:396.513
Hs Code.:

Synonyms:N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

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Chemical Property of N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

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Technology Process of N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

There total 8 articles about N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300749-30-7
C₂₁H₂₂N₄O₂S

: 1300749-25-0
N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: C₂₁H₂₂N₄O₂S

: 1300749-25-0
N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: 220378-49-4
C₈H₁₃N₃O₃S

: 1300749-25-0
N-benzhydryl-N-((2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-2-propenyl) amine

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: hydrazine hydrate / ethanol / 3 h / Inert atmosphere; Reflux

4: ethanol / 20 °C / Inert atmosphere

5: sodium tetrahydroborate / methanol / 3 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; thionyl chloride; hydrazine hydrate; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00657b