2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle

Base Information

Chemical Name:2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle
CAS No.:129625-08-7
Molecular Formula:C₂₄H₂₂N₂O₅
Molecular Weight:418.449
Hs Code.:

Synonyms:2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle

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Chemical Property of 2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle

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Technology Process of 2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle

There total 3 articles about 2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 617-52-7
Dimethyl itakonate

: 68001-26-3
fluoroborate de 2-benzoyl-1,2-dihydroisoquinaldonitrile

: 129625-08-7
2-(1-isoquinoleinyl)-3-methoxycarbonylmethyl-5-hydroxy-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylate de methyle

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 4h;

Reference yield:

: 617-52-7
Dimethyl itakonate

: 129625-08-7
(3S,5R)-5-Hydroxy-2-isoquinolin-1-yl-3-methoxycarbonylmethyl-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / NEt₃ / dimethylformamide / 4 h / 0 °C

2: H(+) / CDCl₃

With hydrogen cation; triethylamine; In chloroform-d1; N,N-dimethyl-formamide;

Reference yield:

: 68001-26-3
fluoroborate de 2-benzoyl-1,2-dihydroisoquinaldonitrile

: 129625-08-7
(3S,5R)-5-Hydroxy-2-isoquinolin-1-yl-3-methoxycarbonylmethyl-5-phenyl-4,5-dihydro-3H-pyrrole-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / NEt₃ / dimethylformamide / 4 h / 0 °C

2: H(+) / CDCl₃

With hydrogen cation; triethylamine; In chloroform-d1; N,N-dimethyl-formamide;