trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum

Base Information

• Chemical Name: trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum
• CAS No.: 65498-66-0
• Molecular Formula: C₅₂H₅₀MoN₄P₄
• Molecular Weight: 950.831

Synonyms:trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum

Chemical Property of trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum

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Technology Process of trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum

There total 3 articles about trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

Mo(N2)2(PPh2Me)4 (33248-03-2,66008-09-1,115461-51-3) + 1,2-bis-(diphenylphosphino)ethane (1663-45-2) → trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum (65498-66-0)

Guidance literature:

In benzene; to soln. Mo(N2)2(PPh2Me)4 in benzene dppe added and mixt. stirred for 2h; chilled methanol at 0°C added and mixt. allowed to stand in 5°C refrigerator for 16 h, solid filtered, washed with methanol and dried in vacuo; elem. anal.;

DOI:10.1021/ic50215a061

Reference yield:

trans-bis(dinitrogen)(PMePh2)4 molybdenum → trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum (65498-66-0)

Guidance literature:

With 1,2-bis(diphenylphosphino)ethane; In not given;

DOI:10.1039/DT9770001852

Reference yield:

MoCl4(dppe) (40219-67-8) + magnesium (7439-95-4) + diphenyl(methyl)phosphine (1486-28-8) → trans-[1,2-bis(diphenylphosphino)ethane]bis(dinitrogen)bis(methyldiphenylphosphine)molybdenum (65498-66-0)

Guidance literature:

With N₂; In tetrahydrofuran; stirring under N2;

DOI:10.1039/DT9770002139

upstream raw materials:

Mo(N₂)₂(PPh₂Me)₄

1,2-bis-(diphenylphosphino)ethane

MoCl₄(dppe)

magnesium

Downstream raw materials:

nitrogen

MoBr₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(P(C₆H₅)2(CH₃))

hydrazine

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