4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

Base Information

Chemical Name:4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid
CAS No.:177845-97-5
Molecular Formula:C₁₁H₁₁BrO₄
Molecular Weight:287.11
Hs Code.:

Synonyms:4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

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Chemical Property of 4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

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Technology Process of 4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

There total 7 articles about 4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2-(4-Bromo-phenyl)-2-carboxy-pentanedioic acid

: 177845-97-5
4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

Guidance literature:: With sulfuric acid; In water; for 2h; Heating;
DOI:10.1002/(SICI)1099-1344(199605)38:5<425::AID-JLCR860>3.0.CO;2-B

Reference yield: 89.0%

: 201230-82-2
carbon monoxide

: 58824-56-9
1-(p-bromophenyl)prop-2-en-1-ol

: 177845-97-5
4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

Guidance literature:: With HeMaRaphos; water; toluene-4-sulfonic acid; palladium dichloride; In tetrahydrofuran; at 125 ℃; for 24h; under 30003 Torr; regioselective reaction; Autoclave; Green chemistry;
DOI:10.1002/anie.202008916

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 177845-97-5
4-(4'-bromophenyl)-4-hydroxycarbonylbutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 h / 20 °C

2: HeMaRaphos; water; palladium dichloride; toluene-4-sulfonic acid / tetrahydrofuran / 24 h / 125 °C / 30003 Torr / Autoclave; Green chemistry

With HeMaRaphos; water; toluene-4-sulfonic acid; palladium dichloride; In tetrahydrofuran;
DOI:10.1002/anie.202008916