N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide

Base Information

• Chemical Name: N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide
• CAS No.: 1501972-45-7
• Molecular Formula: C₁₉H₂₃IN*I
• Molecular Weight: 519.207
• Mol file: 1501972-45-7.mol

Synonyms:N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide

Chemical Property of N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide

There total 4 articles about N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

diiodomethane (75-11-6) + DHP-362 (46970-87-0) → N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide (1501972-45-7)

Guidance literature:

In acetonitrile; at 20 ℃; for 24h; Darkness;

DOI:10.3390/molecules21040381

Reference yield:

phenylmagnesium bromide (100-58-3) → N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide (1501972-45-7)

Guidance literature:

Multi-step reaction with 4 steps

1: diethyl ether / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / benzene / 6 h / Dean-Stark; Reflux

3: water; tetrahydrofuran / 20 °C

4: acetonitrile / 24 h / 20 °C / Darkness

With toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; water; acetonitrile; benzene; 1: |Grignard Reaction;

DOI:10.3390/molecules21040381

Reference yield:

4-bromo-1,1-diphenylbutanol (114736-30-0) → N-iodomethyl-N,N-dimethyl-N-(4,4-diphenylbut-3-en-1-yl)ammonium iodide (1501972-45-7)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / benzene / 6 h / Dean-Stark; Reflux

2: water; tetrahydrofuran / 20 °C

3: acetonitrile / 24 h / 20 °C / Darkness

With toluene-4-sulfonic acid; In tetrahydrofuran; water; acetonitrile; benzene;

DOI:10.3390/molecules21040381

upstream raw materials:

diiodomethane

DHP-362

phenylmagnesium bromide

4-bromo-1,1-diphenylbutanol