[(C₆H₂Cl₂(S)2)Fe(CO)(P(C₆H₅)2CH₂N(CH₂CF₃)CH₂P(C₆H₅)2)]

Base Information

• Chemical Name: [(C₆H₂Cl₂(S)2)Fe(CO)(P(C₆H₅)2CH₂N(CH₂CF₃)CH₂P(C₆H₅)2)]
• CAS No.: 1351395-74-8
• Molecular Formula: C₃₅H₂₈Cl₂F₃FeNOP₂S₂
• Molecular Weight: 788.441
• Mol file: 1351395-74-8.mol

Synonyms:[(C₆H₂Cl₂(S)2)Fe(CO)(P(C₆H₅)2CH₂N(CH₂CF₃)CH₂P(C₆H₅)2)]

Chemical Property of [(C₆H₂Cl₂(S)2)Fe(CO)(P(C₆H₅)2CH₂N(CH₂CF₃)CH₂P(C₆H₅)2)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(C₆H₂Cl₂(S)2)Fe(CO)(P(C₆H₅)2CH₂N(CH₂CF₃)CH₂P(C₆H₅)2)]

There total 2 articles about [(C₆H₂Cl₂(S)2)Fe(CO)(P(C₆H₅)2CH₂N(CH₂CF₃)CH₂P(C₆H₅)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-dichlorobenzene-1,2-dithiol (87314-49-6) + carbon monoxide (201230-82-2) + (C6H5)2PCH2N(CH2CF3)CH2P(C6H5)2 (246873-78-9) + iron(II) chloride → [(C6H2Cl2(S)2)Fe(CO)(P(C6H5)2CH2N(CH2CF3)CH2P(C6H5)2)] (1351395-74-8)

Guidance literature:

With Et₃N; In methanol; react. of Fe salt with (PPh2CH2)2NCH2CF3 and C6H2Cl2(SH)2 in CH3OH underCO atm. at room temp. for 1 h;

DOI:10.1039/c1cc14449a

Reference yield:

(C6H5)2PCH2N(CH2CF3)CH2P(C6H5)2 (246873-78-9) + Fe2(CO)6(C6H2Cl2S2) → [(C6H2Cl2(S)2)Fe(CO)(P(C6H5)2CH2N(CH2CF3)CH2P(C6H5)2)] (1351395-74-8)

Guidance literature:

With Me₃NO*2H₂O; In acetonitrile; react. of Fe complex with Me3NO in CH3CN at room temp. for 15 min; then with CF3H2N(CH2PPh2)2 in CH3CN at room temp. for 1 h;

DOI:10.1039/c1cc14449a

upstream raw materials:

3,6-dichlorobenzene-1,2-dithiol

carbon monoxide

(C₆H₅)2PCH₂N(CH₂CF₃)CH₂P(C₆H₅)2