Technology Process of C12H14O3
There total 4 articles about C12H14O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(2'R,4R,Z)-N-(4'-benzyloxyl-2-methylbut-3'-enoyl)-4,5,5-triphenyloxazolidin-2-one;
With
dihydrogen peroxide; lithium hydroxide;
In
tetrahydrofuran; water;
at 0 - 25 ℃;
for 1.3h;
With
potassium hydrogensulfate; sodium sulfite;
In
tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2012.06.133
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pivaloyl chloride / tetrahydrofuran / 18 h / 0 - 25 °C
2.1: potassium hexamethylsilazane; lithium chloride / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere
2.2: 7 h / -60 - -45 °C / Inert atmosphere
2.3: Inert atmosphere; Saturated solution
3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.3 h / 0 - 25 °C
With
dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; lithium chloride; lithium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2012.06.133
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hexamethylsilazane; lithium chloride / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere
1.2: 7 h / -60 - -45 °C / Inert atmosphere
1.3: Inert atmosphere; Saturated solution
2.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.3 h / 0 - 25 °C
With
dihydrogen peroxide; potassium hexamethylsilazane; lithium chloride; lithium hydroxide;
In
tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2012.06.133
