C₃₀H₄₆N₂O₆SSi

Base Information

Chemical Name:C₃₀H₄₆N₂O₆SSi
CAS No.:956219-58-2
Molecular Formula:C₃₀H₄₆N₂O₆SSi
Molecular Weight:590.857
Hs Code.:

C<sub>30</sub>H<sub>46</sub>N<sub>2</sub>O<sub>6</sub>SSi

Synonyms:C₃₀H₄₆N₂O₆SSi

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Chemical Property of C₃₀H₄₆N₂O₆SSi

Chemical Property:

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Technology Process of C₃₀H₄₆N₂O₆SSi

There total 18 articles about C₃₀H₄₆N₂O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: C₂₁H₂₆N₂O₆S

: 956219-58-2
C₃₀H₄₆N₂O₆SSi

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jo9817117

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 956219-58-2
C₃₀H₄₆N₂O₆SSi

Guidance literature:: Multi-step reaction with 18 steps

1.1: Ph₃P; DEAD / tetrahydrofuran

2.1: n-BuLi / diethyl ether

3.1: H₂ / Pd/CaCO₃/Pb / toluene

4.1: lithium hexamethyldisilazane / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

4.2: 71 percent / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

5.1: 69 percent / dimethylsulfoxide / 180 °C

6.1: 91 percent / Me₃Al / toluene

7.1: LHMDS / tetrahydrofuran / -78 °C

7.2: 79 percent / N,N-dimethylpropylene urea / tetrahydrofuran / -78 °C

8.1: 75 percent / aq. HCl / tetrahydrofuran

9.1: 98 percent / DMAP / acetonitrile

10.1: DIBALH / CH₂Cl₂ / -78 °C

11.1: NaCNBH₃ / acetic acid

12.1: TBAF / tetrahydrofuran

13.1: K₂CO₃ / methanol

14.1: DIBALH / CH₂Cl₂ / -78 °C

14.2: 78 percent / aq. HCl

15.1: 90 percent / sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

16.1: BH₃*THF / tetrahydrofuran / 0 °C

16.2: NaOH; H₂O₂ / tetrahydrofuran; ethanol; H₂O

17.1: Dess-Martin periodinane / CH₂Cl₂ / 0 °C

18.1: 77 percent / Et₃N / CH₂Cl₂ / 0 °C

With hydrogenchloride; dmap; n-butyllithium; borane-THF; tetrabutyl ammonium fluoride; hydrogen; trimethylaluminum; sodium hexamethyldisilazane; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; triethylamine; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate; Lindlar's catalyst; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; acetic acid; dimethyl sulfoxide; toluene; acetonitrile; 1.1: Alkylation / 2.1: Acylation / 3.1: Catalytic hydrogenation / 4.1: Metallation / 4.2: Michael addition / 5.1: Elimination / 6.1: Cyclization / 7.1: Metallation / 7.2: Alkylation / 8.1: Hydrolysis / 9.1: Acylation / 10.1: Reduction / 11.1: Reduction / 12.1: desilylation / 13.1: Cyclization / 14.1: Reduction / 14.2: Cyclization / 15.1: Cyclization / 16.1: Addition / 16.2: Oxidation / 17.1: Oxidation / 18.1: silylation;
DOI:10.1021/jo9817117

Reference yield:

: 338463-00-6
N-(tert-butoxycarbonyl)-N-but-3-ynyl-4-methylbenzenesulfonamide

: 956219-58-2
C₃₀H₄₆N₂O₆SSi

Guidance literature:: Multi-step reaction with 17 steps

1.1: n-BuLi / diethyl ether

2.1: H₂ / Pd/CaCO₃/Pb / toluene

3.1: lithium hexamethyldisilazane / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

3.2: 71 percent / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

4.1: 69 percent / dimethylsulfoxide / 180 °C

5.1: 91 percent / Me₃Al / toluene

6.1: LHMDS / tetrahydrofuran / -78 °C

6.2: 79 percent / N,N-dimethylpropylene urea / tetrahydrofuran / -78 °C

7.1: 75 percent / aq. HCl / tetrahydrofuran

8.1: 98 percent / DMAP / acetonitrile

9.1: DIBALH / CH₂Cl₂ / -78 °C

10.1: NaCNBH₃ / acetic acid

11.1: TBAF / tetrahydrofuran

12.1: K₂CO₃ / methanol

13.1: DIBALH / CH₂Cl₂ / -78 °C

13.2: 78 percent / aq. HCl

14.1: 90 percent / sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

15.1: BH₃*THF / tetrahydrofuran / 0 °C

15.2: NaOH; H₂O₂ / tetrahydrofuran; ethanol; H₂O

16.1: Dess-Martin periodinane / CH₂Cl₂ / 0 °C

17.1: 77 percent / Et₃N / CH₂Cl₂ / 0 °C

With hydrogenchloride; dmap; n-butyllithium; borane-THF; tetrabutyl ammonium fluoride; hydrogen; trimethylaluminum; sodium hexamethyldisilazane; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; triethylamine; lithium hexamethyldisilazane; Lindlar's catalyst; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; acetic acid; dimethyl sulfoxide; toluene; acetonitrile; 1.1: Acylation / 2.1: Catalytic hydrogenation / 3.1: Metallation / 3.2: Michael addition / 4.1: Elimination / 5.1: Cyclization / 6.1: Metallation / 6.2: Alkylation / 7.1: Hydrolysis / 8.1: Acylation / 9.1: Reduction / 10.1: Reduction / 11.1: desilylation / 12.1: Cyclization / 13.1: Reduction / 13.2: Cyclization / 14.1: Cyclization / 15.1: Addition / 15.2: Oxidation / 16.1: Oxidation / 17.1: silylation;
DOI:10.1021/jo9817117