C₃₂H₄₃N₇O₄

Base Information

Chemical Name:C₃₂H₄₃N₇O₄
CAS No.:1346245-59-7
Molecular Formula:C₃₂H₄₃N₇O₄
Molecular Weight:589.738
Hs Code.:

C<sub>32</sub>H<sub>43</sub>N<sub>7</sub>O<sub>4</sub>

Synonyms:C₃₂H₄₃N₇O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₄₃N₇O₄

Chemical Property:

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Technology Process of C₃₂H₄₃N₇O₄

There total 9 articles about C₃₂H₄₃N₇O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1346245-58-6
C₃₀H₃₈N₆O₇S

: 75-31-0
isopropylamine

: 1346245-59-7
C₃₂H₄₃N₇O₄

Guidance literature:: In acetonitrile; at 100 ℃; for 18h; sealed vessel;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1346245-59-7
C₃₂H₄₃N₇O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / 1,2-dimethoxyethane; water / 1 h / 60 °C

1.2: 0.5 h / 60 °C

2.1: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

3.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 72 h / 85 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

4.2: Cooling with ice

5.1: triethylamine / dichloromethane / 3 h / 5 - 20 °C / Inert atmosphere

6.1: acetonitrile / 18 h / 100 °C / sealed vessel

With 1H-imidazole; tetrabutyl ammonium fluoride; caesium carbonate; triethylamine; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetonitrile;

Reference yield:

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1346245-59-7
C₃₂H₄₃N₇O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 5 °C / Inert atmosphere

1.2: 18 h / 5 - 20 °C / Inert atmosphere

2.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 72 h / 85 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.2: Cooling with ice

4.1: triethylamine / dichloromethane / 3 h / 5 - 20 °C / Inert atmosphere

5.1: acetonitrile / 18 h / 100 °C / sealed vessel

With tetrabutyl ammonium fluoride; sodium hydride; caesium carbonate; triethylamine; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;