C₄₅H₃₇N₃O₈

Base Information

• Chemical Name: C₄₅H₃₇N₃O₈
• CAS No.: 244128-10-7
• Molecular Formula: C₄₅H₃₇N₃O₈
• Molecular Weight: 747.804
• Mol file: 244128-10-7.mol

Synonyms:C₄₅H₃₇N₃O₈

Chemical Property of C₄₅H₃₇N₃O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₃₇N₃O₈

There total 1 articles about C₄₅H₃₇N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C45H38BrN3O8 (244128-09-4) → C45H37N3O8 (244128-10-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 23 ℃; for 5h; Irradiation;

DOI:10.1021/ja990909l

Reference yield:

C45H37N3O8 (244128-10-7) → C33H27N3O5Se

Guidance literature:

Multi-step reaction with 5 steps

1: 97 percent / KOH / H₂O; methanol; tetrahydrofuran / 0.75 h / 23 °C

2: 82 percent / I₂, Ph₃P, imidazole / tetrahydrofuran / 1 h / 23 °C

3: 93 percent / NaBH₄ / ethanol; tetrahydrofuran / 23 °C

4: 98 percent / Py, DMAP / 0.17 h / 23 °C

5: m-CPBA / tetrahydrofuran / 0.17 h / 23 °C

With pyridine; 1H-imidazole; dmap; potassium hydroxide; sodium tetrahydroborate; iodine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; water;

DOI:10.1021/ja990909l

Reference yield:

C45H37N3O8 (244128-10-7) → C31H25N3O3Se (244128-13-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 97 percent / KOH / H₂O; methanol; tetrahydrofuran / 0.75 h / 23 °C

2: 82 percent / I₂, Ph₃P, imidazole / tetrahydrofuran / 1 h / 23 °C

3: 93 percent / NaBH₄ / ethanol; tetrahydrofuran / 23 °C

With 1H-imidazole; potassium hydroxide; sodium tetrahydroborate; iodine; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; water;

DOI:10.1021/ja990909l

upstream raw materials:

C₄₅H₃₈BrN₃O₈

Downstream raw materials:

K-252a

K-252b

C₃₁H₂₅N₃O₃Se

C₃₃H₂₇N₃O₄Se