Technology Process of 6-phenylhexane-1-sulfonyl fluoride
There total 3 articles about 6-phenylhexane-1-sulfonyl fluoride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dimanganese decacarbonyl; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate;
In
dimethyl sulfoxide;
at 20 ℃;
for 24h;
Inert atmosphere;
Irradiation;
DOI:10.1002/adsc.202000515
- Guidance literature:
-
With
ammonium fluoride;
In
acetone;
Reflux;
DOI:10.1021/jm301205j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triphenylphosphine; 1H-imidazole; iodine / acetonitrile; diethyl ether / 0 - 20 °C / Inert atmosphere
2.1: tert.-butyl lithium / diethyl ether; pentane; hexane / 0.17 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 °C / Inert atmosphere
3.1: ammonium fluoride / acetone / Reflux
With
1H-imidazole; ammonium fluoride; iodine; tert.-butyl lithium; triphenylphosphine;
In
diethyl ether; hexane; acetone; acetonitrile; pentane;
DOI:10.1021/jm301205j
