3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

Base Information

• Chemical Name: 3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide
• CAS No.: 583844-03-5
• Molecular Formula: C₂₃H₃₀N₂O₈
• Molecular Weight: 462.5

Synonyms:3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

Chemical Property of 3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

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Technology Process of 3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

There total 1 articles about 3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H26N2O8 → 3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH2O-acetonide (583844-03-5)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; water; for 4h;

Reference yield:

3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH2O-acetonide (583844-03-5) + benzyl bromide (100-39-0) → C30H36N2O8 + 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH2O-acetonide (583844-04-6)

Guidance literature:

3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 0.25h;

benzyl bromide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 7h;

Downstream raw materials:

5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

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