(R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ⁴-thiazolidine-4r-carboxylic acid methylamide

Base Information

• Chemical Name: (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ⁴-thiazolidine-4r-carboxylic acid methylamide
• CAS No.: 57001-75-9
• Molecular Formula: C₁₉H₁₈N₂O₃S
• Molecular Weight: 354.43

Synonyms:(R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ⁴-thiazolidine-4r-carboxylic acid methylamide

Chemical Property of (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ⁴-thiazolidine-4r-carboxylic acid methylamide

Chemical Property:

Purity/Quality:

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Technology Process of (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ⁴-thiazolidine-4r-carboxylic acid methylamide

There total 3 articles about (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ⁴-thiazolidine-4r-carboxylic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-3-benzoyl-2-(Z)-benzylidene-thiazolidine-4-carboxylic acid methylamide (57001-74-8) → (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ4-thiazolidine-4r-carboxylic acid methylamide (57001-75-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ja00850a043

Reference yield:

benzoyl chloride (98-88-4) → (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ4-thiazolidine-4r-carboxylic acid methylamide (57001-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N

2: MCPBA / CH₂Cl₂

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ja00850a043

Reference yield:

(R)-2-benzyl-4,5-dihydro-thiazole-4-carboxylic acid methylamide (57001-73-7) → (R)-3-benzoyl-2-(Z)-benzylidene-1ξ-oxo-1λ4-thiazolidine-4r-carboxylic acid methylamide (57001-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N

2: MCPBA / CH₂Cl₂

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ja00850a043

upstream raw materials:

(R)-3-benzoyl-2-(Z)-benzylidene-thiazolidine-4-carboxylic acid methylamide

benzoyl chloride

(R)-2-benzyl-4,5-dihydro-thiazole-4-carboxylic acid methylamide

Downstream raw materials:

(4R)-5c-acetoxy-3-benzoyl-2-(Z)-benzylidene-thiazolidine-4r-carboxylic acid methylamide

(4R)-5t-acetoxy-3-benzoyl-2-(Z)-benzylidene-thiazolidine-4r-carboxylic acid methylamide

2-benzyl-thiazole-4-carboxylic acid methylamide

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