Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

Base Information

Chemical Name:Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester
CAS No.:457653-78-0
Molecular Formula:C₃₂H₅₆O₄
Molecular Weight:504.794
Hs Code.:

Synonyms:Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

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Chemical Property of Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

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Technology Process of Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

There total 2 articles about Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 334-48-5
1-decanoic acid

: 90904-31-7
(S)-1-Benzyloxy-3-dodecyloxy-propan-2-ol

: 457653-78-0
Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/ol026039l

Reference yield:

: 17325-85-8
(2S)-3-(benzyloxy)propane-1,2-diol

: 457653-78-0
Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-n-butylammonium hydrogen sulfate; sodium hydroxide / benzene / 45 °C

2: 85 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂

With dmap; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; dicyclohexyl-carbodiimide; In dichloromethane; benzene;
DOI:10.1021/ol026039l

Reference yield:

: 457653-78-0
Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

: 457653-79-1
Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 10percent Pd/C

2: sodium hypochlorite; 4-acetamido-2,2,6,6-tetramethyl-1-piperidinyloxy radical; sodium bromide / toluene; ethyl acetate; H₂O / -10 °C

3: tetrahydrofuran / 65 °C

With 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium hypochlorite; hydrogen; sodium bromide; 10percent Pd/C; In tetrahydrofuran; water; ethyl acetate; toluene;
DOI:10.1021/ol026039l