Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

Base Information

Chemical Name:Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester
CAS No.:457653-79-1
Molecular Formula:C₃₄H₅₆O₅
Molecular Weight:544.816
Hs Code.:

Synonyms:Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

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Chemical Property of Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

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Technology Process of Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

There total 4 articles about Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90904-31-7
(S)-1-Benzyloxy-3-dodecyloxy-propan-2-ol

: 457653-79-1
Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂

2: hydrogen / 10percent Pd/C

3: sodium hypochlorite; 4-acetamido-2,2,6,6-tetramethyl-1-piperidinyloxy radical; sodium bromide / toluene; ethyl acetate; H₂O / -10 °C

4: tetrahydrofuran / 65 °C

With dmap; 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium hypochlorite; hydrogen; dicyclohexyl-carbodiimide; sodium bromide; 10percent Pd/C; In tetrahydrofuran; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/ol026039l

Reference yield:

: 457653-78-0
Decanoic acid (S)-2-benzyloxy-1-dodecyloxymethyl-ethyl ester

: 457653-79-1
Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 10percent Pd/C

2: sodium hypochlorite; 4-acetamido-2,2,6,6-tetramethyl-1-piperidinyloxy radical; sodium bromide / toluene; ethyl acetate; H₂O / -10 °C

3: tetrahydrofuran / 65 °C

With 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium hypochlorite; hydrogen; sodium bromide; 10percent Pd/C; In tetrahydrofuran; water; ethyl acetate; toluene;
DOI:10.1021/ol026039l

Reference yield:

: Decanoic acid (R)-2-dodecyloxy-1-hydroxymethyl-ethyl ester

: 457653-79-1
Decanoic acid (E)-(R)-3-benzyloxycarbonyl-1-dodecyloxymethyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hypochlorite; 4-acetamido-2,2,6,6-tetramethyl-1-piperidinyloxy radical; sodium bromide / toluene; ethyl acetate; H₂O / -10 °C

2: tetrahydrofuran / 65 °C

With 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium hypochlorite; sodium bromide; In tetrahydrofuran; water; ethyl acetate; toluene;
DOI:10.1021/ol026039l