Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside
CAS No.:139760-32-0
Molecular Formula:C₆₂H₆₇NO₂₁
Molecular Weight:1162.21
Hs Code.:

Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Synonyms:Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Chemical Property of Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Technology Process of Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

There total 10 articles about Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.5%

: 139760-22-8
Methyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 139760-08-0
O-(2,3,4-Tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-galactopyranosyl chloride

: 139760-37-5
Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 139760-32-0
Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver perchlorate; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jo00034a047

Reference yield:

: 100-39-0
benzyl bromide

: 139760-32-0
Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 79.2 percent / KOH / dimethylsulfoxide / 4 h / Ambient temperature

2: 95 percent / ceric ammonium nitrate (CAN) / acetonitrile; H₂O / 0.33 h / Ambient temperature

3: 47.5 percent / 2,4,6-trimethylpyridine, AgClO₄ / CH₂Cl₂ / 4 h / Ambient temperature

With 2,4,6-trimethyl-pyridine; potassium hydroxide; ammonium cerium(IV) nitrate; silver perchlorate; In dichloromethane; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/jo00034a047

Reference yield:

: 139760-20-6
Methyl 2-acetamido-2-deoxy-3-O-(p-methoxybenzyl)-α-D-glucopyranoside

: 139760-32-0
Methyl O-(2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 79.2 percent / KOH / dimethylsulfoxide / 4 h / Ambient temperature

2: 95 percent / ceric ammonium nitrate (CAN) / acetonitrile; H₂O / 0.33 h / Ambient temperature

3: 47.5 percent / 2,4,6-trimethylpyridine, AgClO₄ / CH₂Cl₂ / 4 h / Ambient temperature

With 2,4,6-trimethyl-pyridine; potassium hydroxide; ammonium cerium(IV) nitrate; silver perchlorate; In dichloromethane; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/jo00034a047