Technology Process of C30H41N3O3
There total 10 articles about C30H41N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol; water;
at 20 ℃;
for 12h;
DOI:10.1021/ml300083p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / tetrahydrofuran; water / 0.5 h / 80 °C / Inert atmosphere; Microwave irradiation
2: sodium hydroxide / methanol; water / 12 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; methanol; water;
1: |Suzuki Coupling;
DOI:10.1021/ml300083p
- Guidance literature:
-
Multi-step reaction with 8 steps
1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 7 h / Reflux
2: 5 h / Inert atmosphere; Reflux
3: lithium diisopropyl amide / tetrahydrofuran / 12 h / -78 - 20 °C
4: bromine; potassium carbonate / dichloromethane / 1.5 h / 0 - 20 °C
5: sodium hydroxide / methanol / 3 h / 40 °C
6: dmap; thionyl chloride / dichloromethane / 12 h / -20 - 20 °C
7: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / tetrahydrofuran; water / 0.5 h / 80 °C / Inert atmosphere; Microwave irradiation
8: sodium hydroxide / methanol; water / 12 h / 20 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; thionyl chloride; 2,2'-azobis(isobutyronitrile); bromine; potassium carbonate; sodium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water;
3: |Wittig-Horner Reaction / 7: |Suzuki Coupling;
DOI:10.1021/ml300083p