3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

Base Information

Chemical Name:3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine
CAS No.:1422006-17-4
Molecular Formula:C₅₄H₄₁NO₃P₂
Molecular Weight:813.872
Hs Code.:

Synonyms:3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

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Chemical Property of 3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

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Technology Process of 3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

There total 1 articles about 3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 267221-88-5
4-(diphenylamino)phenylboronic pinacol ester

: 1420904-83-1
4-bromo-2-(diphenylphosphinoyl)-1-[2-(diphenylphosphinoyl)phenoxy]benzene

: 1422006-17-4
3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; In tetrahydrofuran; water; at 80 ℃; for 24h; Alkaline conditions; Inert atmosphere;
DOI:10.1021/cm403160p

Reference yield: 66.0%

: 326-91-0
1,1,1-trifluoro-4-(2-thienyl)butane-2,4-dione

: europium(III) chloride hexahydrate

: 1422006-17-4
3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

: [Eu(4,4,4-trifluoro-1-(thiophen-2-yl)butane-1,3-dione)₃bis(2-(diphenylphosphino)phenyl)ether oxide(triphenylamine)]

Guidance literature:: 1,1,1-trifluoro-4-(2-thienyl)butane-2,4-dione; europium(III) chloride hexahydrate; With sodium hydroxide; In ethanol; water; at 70 ℃; for 0.5h;

3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine; In ethanol; water; at 70 ℃; for 8h;
DOI:10.1002/chem.201403244

Reference yield: 65.0%

: europium(III) chloride hexahydrate

: 1422006-17-4
3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine

: 120-46-7,61346-73-4
1,3-diphenylpropanedione

: [Eu(1,3-diphenylpropane-1,3-dione)₃bis(2-(diphenylphosphino)phenyl)ether oxide(triphenylamine)]

Guidance literature:: europium(III) chloride hexahydrate; 1,3-diphenylpropanedione; With sodium hydroxide; In ethanol; water; at 70 ℃; for 0.5h;

3′-(diphenylphosphoryl)-4′-(2-(diphenylphosphoryl)phenoxy)-N,N-diphenylbiphenyl-4-amine; In ethanol; water; at 70 ℃; for 8h;
DOI:10.1002/chem.201403244