(+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Base Information

Chemical Name:(+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile
CAS No.:102311-65-9
Molecular Formula:C₂₁H₁₈N₂O₃
Molecular Weight:346.386
Hs Code.:

(+/-)-2-<i>trans</i>-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Synonyms:(+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Suppliers and Price of (+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

There total 3 articles about (+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 102311-65-9
(+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: palladium/charcoal; decalin

2: benzene

With palladium on activated charcoal; decalin; benzene;
DOI:10.1021/ja01571a043

Reference yield:

: 15248-39-2
6,7-dimethoxyisoquinoline

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 102311-65-9
(+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Guidance literature:: With benzene;
DOI:10.1021/ja01571a043

Reference yield:

: 58163-19-2
dimethoxy-3,4 benzylideneaminoacetal diethylique

: 102311-65-9
(+/-)-2-trans-cinnamoyl-6,7-dimethoxy-1,2-dihydro-isoquinoline-1-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: phosphoryl chloride; polyphosphoric acid / 23 - 26 °C

2: benzene

With PPA; trichlorophosphate; benzene;
DOI:10.1021/ja01571a043