[(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl₂

Base Information

• Chemical Name: [(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl₂
• CAS No.: 1041851-96-0
• Molecular Formula: C₃₀H₂₈Cl₂F₁₂N₂O₂Ti
• Molecular Weight: 795.331
• Mol file: 1041851-96-0.mol

Synonyms:[(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl₂

Chemical Property of [(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl₂

There total 1 articles about [(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(p-C6H4CF3)NC(trifluoromethyl)CHC(tert-butyl)OH (1041851-77-7) + titanium tetrachloride (7550-45-0) → [(p-C6H4CF3)NC(trifluoromethyl)CHC(tert-butyl)O]2TiCl2 (1041851-96-0)

Guidance literature:

With n-butyllithium; In diethyl ether; hexane; (Ar); using Schlenk techniques; addn. of BuLi/hexane to stirred soln. ofp-CF3C6H4NCCF3CHC4H9COH/Et2O at -78°C for 5 min; warming to room temp., stirring for 2.5 h; addn. to TiCl4/Et2O at -78°C for 0.5 h; stirring overnight at room temp.; evapn. of solvent under vac., addn. of hexane; stirring for 10 min at 60°C; filtration, slow cooling to -35°C; crystn., elem. anal.;

DOI:10.1021/om700803u

upstream raw materials:

(p-C₆H₄CF₃)NC(trifluoromethyl)CHC(tert-butyl)OH

titanium tetrachloride