C₅₃H₇₃N₁₁O₇

Base Information

Chemical Name:C₅₃H₇₃N₁₁O₇
CAS No.:1427038-84-3
Molecular Formula:C₅₃H₇₃N₁₁O₇
Molecular Weight:976.232
Hs Code.:

C<sub>53</sub>H<sub>73</sub>N<sub>11</sub>O<sub>7</sub>

Synonyms:C₅₃H₇₃N₁₁O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₇₃N₁₁O₇

Chemical Property:

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Technology Process of C₅₃H₇₃N₁₁O₇

There total 13 articles about C₅₃H₇₃N₁₁O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-15-7,931-16-8,6850-38-0,6982-39-4,33092-82-9,38898-70-3,74111-21-0,108267-20-5
(1S,2S)-trans-2-aminocyclohexanol

: 1427038-84-3
C₅₃H₇₃N₁₁O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium carbonate; acetic anhydride / water; acetone / 3 h / 0 - 20 °C

1.2: 3 h / 0 - 20 °C

1.3: 1 h / Reflux; Enzymatic reaction

2.1: sodium hydroxide / water; 1,4-dioxane / 0 °C

3.1: triethylamine / dichloromethane / 0 h / 0 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

5.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

5.2: 2 h / 4 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

7.1: hydrogen; acetic acid; palladium 10% on activated carbon / methanol / 2 h

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h

9.1: 0.5 h / 0 °C

10.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

With sodium azide; palladium 10% on activated carbon; hydrogen; acetic anhydride; sodium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja401151v

Reference yield:

: 118457-61-7
(1S,2S)-2-azido-1-(trimethylsilyloxy)cyclohexane

: 1427038-84-3
C₅₃H₇₃N₁₁O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: trifluoroacetic acid; platinum(IV) oxide; hydrogen / methanol / 40.5 h / 20 °C

2.1: sodium carbonate; acetic anhydride / water; acetone / 3 h / 0 - 20 °C

2.2: 3 h / 0 - 20 °C

2.3: 1 h / Reflux; Enzymatic reaction

3.1: sodium hydroxide / water; 1,4-dioxane / 0 °C

4.1: triethylamine / dichloromethane / 0 h / 0 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

6.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

6.2: 2 h / 4 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

8.1: hydrogen; acetic acid; palladium 10% on activated carbon / methanol / 2 h

9.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h

10.1: 0.5 h / 0 °C

11.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

With platinum(IV) oxide; sodium azide; palladium 10% on activated carbon; hydrogen; acetic anhydride; sodium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja401151v

Reference yield:

: 214679-17-1,477584-30-8
(1S,2R)-(-)-1-tert-butoxycarbonylaminocyclohexan-2-ol

: 1427038-84-3
C₅₃H₇₃N₁₁O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 0 h / 0 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

3.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

3.2: 2 h / 4 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

5.1: hydrogen; acetic acid; palladium 10% on activated carbon / methanol / 2 h

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h

7.1: 0.5 h / 0 °C

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

With sodium azide; palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja401151v