(1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid

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Chemical Name:(1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid
CAS No.:1234493-10-7
Molecular Formula:C₂₇H₄₀N₂O₇
Molecular Weight:504.624
Hs Code.:

Synonyms:(1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid

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Chemical Property of (1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid

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Technology Process of (1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid

There total 1 articles about (1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1234493-09-4
(S)-tert-butyl 3-((1R,3R)-3-acetyl-2,2-dimethylcyclobutyl)-4-(4-(benzyloxycarbonylamino)butanamido)butanoate

: 1234493-10-7
(1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid

Guidance literature:: With sodium hypobromide; In 1,4-dioxane; water; at -5 ℃; for 5h;
DOI:10.1021/ol1010664

Reference yield: 98.0%

: 1234493-10-7
(1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid

: 4-aminobutyric acid methyl ester trifluoroacetate

: 1234493-11-8
(S)-tert-butyl 4-(4-(benzyloxycarbonylamino)butanamido)-3-((1R,3R)-3-(4-methoxy-4-oxobutylcarbamoyl)-2,2-dimethylcyclobutyl)butanoate

Guidance literature:: (1R,3R)-3-((S)-15,15-dimethyl-3,8,13-trioxo-1-phenyl-2,14-dioxa-4,9-diazahexadecan-11-yl)-2,2-dimethylcyclobutanecarboxylic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.0833333h; Inert atmosphere;

4-aminobutyric acid methyl ester trifluoroacetate; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol1010664