(E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

Base Information

Chemical Name:(E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide
CAS No.:1416978-26-1
Molecular Formula:C₁₉H₁₅Cl₃F₃NO
Molecular Weight:436.688
Hs Code.:

Synonyms:(E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

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Technology Process of (E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

There total 12 articles about (E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1416980-41-0
(E)-(2-chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)phenyl)methanamine

: 64-19-7,77671-22-8
acetic acid

: 1416978-26-1
(E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield: 60.0%

: 2,2,2-trifluoropropanoic acid

: 1416980-41-0
(E)-(2-chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)phenyl)methanamine

: 1416978-26-1
(E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

Guidance literature:: In hexane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 130336-16-2
3,5-dichloro-2,2,2-trifluoroacetophenone

: 1416978-26-1
(E)-N-(2-Chloro-4-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)benzyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate

2: N-Bromosuccinimide / dichloromethane

3: hexane; 1,2-dichloro-benzene; ethyl acetate

4: hydrazine hydrate / dichloromethane; ethanol

5: N,N-dimethyl-formamide; hexane; ethyl acetate

With sodium tetrahydroborate; N-Bromosuccinimide; hydrazine hydrate; In ethanol; hexane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 1,2-dichloro-benzene;