N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

Base Information

Chemical Name:N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine
CAS No.:263342-62-7
Molecular Formula:C₂₄H₂₉BrF₇NO₂Si
Molecular Weight:604.478
Hs Code.:

Synonyms:N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

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Chemical Property of N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

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Technology Process of N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

There total 4 articles about N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 263348-70-5
3-{(3-bromophenyl)[3-(1,1,2,2-tetrafluoroethoxy)benzyl]amino}-1,1,1-trifluoropropan-2-ol

: 263342-62-7
N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/jm020528+

Reference yield:

: 35295-35-3
3-(1,1,2,2-Tetrafluoroethoxy)-benzaldehyde

: 263342-62-7
N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / NaB(OAc)3H; AcOH / 1,2-dichloro-ethane / 1 h / 20 °C

2: Yb(OTf)3 / CH₂Cl₂ / 24 h / 20 °C

3: 3.0 g / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; triethylamine; ytterbium(III) triflate; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm020528+

Reference yield:

: 591-19-5
m-Bromoaniline

: 263342-62-7
N-(3-bromophenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3,3,3-trifluoropropyl]-3-(1,1,2,2-tetrafluoroethoxy)benzenemethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / NaB(OAc)3H; AcOH / 1,2-dichloro-ethane / 1 h / 20 °C

2: Yb(OTf)3 / CH₂Cl₂ / 24 h / 20 °C

3: 3.0 g / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; triethylamine; ytterbium(III) triflate; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm020528+