S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

Base Information

Chemical Name:S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate
CAS No.:1085994-48-4
Molecular Formula:C₁₈H₁₉NOS
Molecular Weight:297.421
Hs Code.:

Synonyms:S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

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Technology Process of S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

There total 6 articles about S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1085994-41-7
(R)-S-ethyl-3-benzyl-4-phenyloxazolidin-2-thionium triflate

: 1085994-48-4
S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

Guidance literature:: (R)-S-ethyl-3-benzyl-4-phenyloxazolidin-2-thionium triflate; With lithium trifluoromethanesulfonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With rubidium iodide; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 - 20 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.3987/COM-08-11410

Reference yield:

: 14231-69-7
(R)-3-benzyl-4-phenyloxazolidine-2-thione

: 1085994-48-4
S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 0.5 h / 20 °C

2.1: lithium trifluoromethanesulfonate / N,N-dimethyl-formamide / 0.5 h / 0 °C / Molecular sieve; Inert atmosphere

2.2: 0 °C / Inert atmosphere

2.3: 0 - 20 °C / Inert atmosphere

With lithium trifluoromethanesulfonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.3987/COM-08-11410

Reference yield:

: 74879-43-9,92850-36-7,142292-44-2,139437-46-0
(R)-N-benzylidene-2-hydroxy-1-phenylethylamine

: 1085994-48-4
S-ethyl N-benzyl-N-1-phenylvinylcarbamothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 0.67 h / 20 °C

2.1: dichloromethane / 5 h / 20 °C

3.1: acetonitrile / 0.5 h / 20 °C

4.1: lithium trifluoromethanesulfonate / N,N-dimethyl-formamide / 0.5 h / 0 °C / Molecular sieve; Inert atmosphere

4.2: 0 °C / Inert atmosphere

4.3: 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; lithium trifluoromethanesulfonate; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3987/COM-08-11410