3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one

Base Information

• Chemical Name: 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one
• CAS No.: 404922-61-8
• Molecular Formula: C₃₀H₃₃NO₂
• Molecular Weight: 439.598

Synonyms:3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one

Chemical Property of 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one

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Technology Process of 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one

There total 6 articles about 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-methyl-benzaldehyde (104-87-0) + dimedone (126-81-8) + aniline (62-53-3) → 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one (404922-61-8)

Guidance literature:

With ferric(III) complex supported on silica coated superparamagnetite iron oxide nanoparticles Fe₃O₄(at)SiO₂ coated by mixture of 3,4-dihydroxybenzaldehyde, barbituric acid, phthalhydrazide; In neat (no solvent); at 80 ℃; for 0.583333h; Green chemistry;

DOI:10.1007/s11164-019-03942-w

Reference yield: 85.0%

5,5-dimethyl-3-(phenylamino)cyclohex-2-en-1-one (18940-21-1) + 4-methyl-benzaldehyde (104-87-0) → 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one (404922-61-8)

Guidance literature:

With LACTIC ACID; In water; at 110 ℃; Sealed tube; Green chemistry;

DOI:10.1002/cjoc.201500195

Reference yield: 81.0%

2,2'-((p-tolyl)methylene)bis(5,5-dimethylcyclohexane-1,3-dione) (351994-01-9) + aniline (62-53-3) → 3,3,6,6-tetramethyl-10-phenyl-9-(p-tolyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-di-one (404922-61-8)

Guidance literature:

With ammonium acetate; acetic acid; for 24h; Reflux;

DOI:10.1002/jhet.2925

upstream raw materials:

4-methyl-benzaldehyde

dimedone

aniline

5,5-dimethyl-3-(phenylamino)cyclohex-2-en-1-one

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