2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol

Base Information

• Chemical Name: 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol
• CAS No.: 97321-68-1
• Molecular Formula: C₄₁H₄₂O₅Se
• Molecular Weight: 693.741

Synonyms:2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol

Chemical Property of 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol

Chemical Property:

Purity/Quality:

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Technology Process of 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol

There total 1 articles about 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-phenylselanylphthalimide (71098-88-9) + 2,3,4,6-Tetra-O-benzyl-D-glucopyranose (4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9) → 2,5-anhydro-3,4,7-tri-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-gulo-heptitol (97321-69-2) + 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol (97321-68-1)

Guidance literature:

With camphor-10-sulfonic acid; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1016/0008-6215(85)85210-1

Reference yield: 97.0%

2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol (97321-68-1) → 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleninyl-D-glycero-D-ido-heptitol (97321-71-6,97372-06-0)

Guidance literature:

With sodium periodate; sodium hydrogencarbonate; In methanol; water; for 2h; Ambient temperature;

DOI:10.1016/0008-6215(85)85210-1

Reference yield: 33.0%

2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleno-D-glycero-D-ido-heptitol (97321-68-1) → 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-D-glycero-D-ido-heptitol (4132-32-5)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tributyl hydride; In toluene; at 90 ℃; for 12h;

DOI:10.1016/0008-6215(85)85210-1

upstream raw materials:

N-phenylselanylphthalimide

2,3,4,6-Tetra-O-benzyl-D-glucopyranose

Downstream raw materials:

2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-D-glycero-D-ido-heptitol

2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-1-phenylseleninyl-D-glycero-D-ido-heptitol

2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-D-gluco-hept-1-enitol

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