N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Base Information

Chemical Name:N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid
CAS No.:74607-96-8
Molecular Formula:C₂₂H₃₀N₂O₄S₃
Molecular Weight:482.689
Hs Code.:

Synonyms:N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

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Chemical Property of N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

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Technology Process of N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

There total 2 articles about N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-40-4
2,4,4-trimethylpent-2-ene

: 851-06-9
bis(p-toluenesulfonyl) sulfur diimide

: 74607-96-8
N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Guidance literature:: at 20 ℃; for 0.2h;

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 74607-96-8
N-<(E)-2,4,4-Trimethyl-2-pentenyl>-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / SOCl₂ / various solvent(s) / 1) 8 h, 80 deg C

2: 96 percent / 0.2 h / 20 °C

With thionyl chloride; In various solvent(s);