C₂₄H₃₀F₃N₅O₃

Base Information

Chemical Name:C₂₄H₃₀F₃N₅O₃
CAS No.:1349113-00-3
Molecular Formula:C₂₄H₃₀F₃N₅O₃
Molecular Weight:493.529
Hs Code.:

C<sub>24</sub>H<sub>30</sub>F<sub>3</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₄H₃₀F₃N₅O₃

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Chemical Property of C₂₄H₃₀F₃N₅O₃

Chemical Property:

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Technology Process of C₂₄H₃₀F₃N₅O₃

There total 5 articles about C₂₄H₃₀F₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₂₂N₂O₂*2ClH

: 1349114-62-0
C₁₃H₁₀F₃N₃O₂

: 1349113-00-3
C₂₄H₃₀F₃N₅O₃

Guidance literature:: C₁₃H₁₀F₃N₃O₂; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

C₁₁H₂₂N₂O₂*2ClH; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1159010-94-2
6-hydroxy-5-methyl-pyrimidine-4-carboxylic acid

: 1349113-00-3
C₂₄H₃₀F₃N₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / 1 h / Reflux

2.1: potassium carbonate / dichloromethane / 1 h / 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine / 2.08 h / 150 °C / 12929 Torr / Microwave irradiation

4.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h / 20 °C

5.2: 20 °C

With thionyl chloride; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1159010-95-3
6-chloro-5-methyl-pyrimidine-4-carboxylic acid chloride

: 1349113-00-3
C₂₄H₃₀F₃N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / dichloromethane / 1 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 2.08 h / 150 °C / 12929 Torr / Microwave irradiation

3.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h / 20 °C

4.2: 20 °C

With water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;