(S)-2-Benzoylamino-N¹-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide

Base Information

• Chemical Name: (S)-2-Benzoylamino-N¹-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide
• CAS No.: 219319-36-5
• Molecular Formula: C₂₈H₃₆N₆O₇
• Molecular Weight: 568.63

Synonyms:(S)-2-Benzoylamino-N¹-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide

Chemical Property of (S)-2-Benzoylamino-N¹-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide

Chemical Property:

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Technology Process of (S)-2-Benzoylamino-N¹-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide

There total 2 articles about (S)-2-Benzoylamino-N¹-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

benzoic acid anhydride (93-97-0) + (S)-2-Amino-N1-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide; compound with trifluoro-acetic acid → (S)-2-Benzoylamino-N1-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide (219319-36-5)

Guidance literature:

With triethylamine; In water; N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1016/S0968-0896(98)00135-7

Reference yield:

{(S)-1-[(S)-5-Benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentylcarbamoyl]-2-carbamoyl-ethyl}-carbamic acid tert-butyl ester (219319-39-8) → (S)-2-Benzoylamino-N1-[(S)-5-benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentyl]-succinamide (219319-36-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / Ambient temperature

2: 81 percent / Et₃N / H₂O; dimethylformamide / Ambient temperature

With triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/S0968-0896(98)00135-7

upstream raw materials:

benzoic acid anhydride

{(S)-1-[(S)-5-Benzoylamino-1-((1S,2R)-1-carbamoyl-2-hydroxy-propylcarbamoyl)-pentylcarbamoyl]-2-carbamoyl-ethyl}-carbamic acid tert-butyl ester

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