Technology Process of ethyl 3,4-di-O-benzyl-2,6-dideoxy-1-C-ethoxy-L-arabino-hexopyranoside
There total 4 articles about ethyl 3,4-di-O-benzyl-2,6-dideoxy-1-C-ethoxy-L-arabino-hexopyranoside which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyrdinium chlorochromate / CH2Cl2 / ultrasound
2: 1) Et3OBF4, 2) Na / multistep reaction; other benzyl ether protected 2-deoxy-aldono-1,5-lactone; synthesis of carbohydrate ortholactones
With
triethyloxonium fluoroborate; sodium; pyridinium chlorochromate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) NaH, DMSO / 1) 1 h, 2) r. t., 3 h
2: pyrdinium chlorochromate / CH2Cl2 / ultrasound
3: 1) Et3OBF4, 2) Na / multistep reaction; other benzyl ether protected 2-deoxy-aldono-1,5-lactone; synthesis of carbohydrate ortholactones
With
triethyloxonium fluoroborate; sodium; sodium hydride; dimethyl sulfoxide; pyridinium chlorochromate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaOMe, MeOH
2: 1) NaH, DMSO / 1) 1 h, 2) r. t., 3 h
3: pyrdinium chlorochromate / CH2Cl2 / ultrasound
4: 1) Et3OBF4, 2) Na / multistep reaction; other benzyl ether protected 2-deoxy-aldono-1,5-lactone; synthesis of carbohydrate ortholactones
With
methanol; sodium methylate; triethyloxonium fluoroborate; sodium; sodium hydride; dimethyl sulfoxide; pyridinium chlorochromate;
In
dichloromethane;