3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate
CAS No.:1159373-67-7
Molecular Formula:C₂₂H₁₉BClF₆NO₇S
Molecular Weight:601.716
Hs Code.:

Synonyms:3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

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Chemical Property of 3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

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Technology Process of 3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

There total 2 articles about 3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2-(2-chlorophenyl)-2-oxoacetyl chloride

: (CF₃)(H₂N)(TfO)C₆H₂B(pinacolate)

: 1159373-67-7
3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 25 ℃;

Reference yield: 84.0%

: 2-(2-chlorophenyl)-2-oxoacetyl chloride

: 1159373-64-4
3-(N,N'-di-tert-butoxycarbonylamino)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

: 76-05-1
trifluoroacetic acid

: 1159373-67-7
3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; treatment of boron compd. with trifluoroacetic acid in CH2Cl2, treatmentof obtained amine deriv. with acyl chloride deriv. in presence of triet hylamine in THF;

Reference yield: 94.0%

: 3587-60-8
Benzyloxymethyl chloride

: 1159373-67-7
3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

: 1159373-68-8
3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; treatment of amide deriv. with benzyloxymethyl chloride in THF in presence of amine deriv.;