3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate
CAS No.:1159373-68-8
Molecular Formula:C₃₀H₂₇BClF₆NO₈S
Molecular Weight:721.867
Hs Code.:

3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Synonyms:3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

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Chemical Property of 3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

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Technology Process of 3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

There total 1 articles about 3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 3587-60-8
Benzyloxymethyl chloride

: 1159373-67-7
3-(2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

: 1159373-68-8
3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; treatment of amide deriv. with benzyloxymethyl chloride in THF in presence of amine deriv.;

Reference yield:

: 1159373-68-8
3-(N-(benzyloxymethyl)-2-(2-chlorophenyl)-2-oxoacetamido)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-(trifluoromethyl)phenyl trifluoromethanesulfonate

: 1159373-69-9
(3S)-1-(benzyloxymethyl)-3-(2-chlorophenyl)-3-hydroxy-2-oxo-4-(trifluoromethyl)indolin-6-yl trifluoromethanesulfonate

: (3R)-1-(benzyloxymethyl)-3-(2-chlorophenyl)-3-hydroxy-2-oxo-4-(trifluoromethyl)indolin-6-yl trifluoromethanesulfonate

Guidance literature:: With CuF*3PPh₃*2EtOH; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; In toluene; at 40 ℃; for 10h; optical yield given as %ee;