methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

Base Information

Chemical Name:methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate
CAS No.:910488-02-7
Molecular Formula:C₂₉H₂₉NO₅
Molecular Weight:471.553
Hs Code.:

Synonyms:methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

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Technology Process of methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

There total 5 articles about methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 910488-02-7
methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

Guidance literature:

Reference yield:

: 5-[(2-benzyloxy-phenanthro[2,3-d][1,3]dioxole-5-carbonyl)-amino]-pentanoic acid methyl ester

: 910488-02-7
methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmc.2006.06.009

Reference yield:

: 910488-32-3
2,3-methyIenedioxy-6-benzyloxy-phenanthrene-9-carboxylic acid

: 910488-02-7
methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine; 1-hydroxybenzotriazole; 4-methylmorpholine / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / dimethylformamide / 0 - 20 °C

2: borane-dimethylsulfide complex / tetrahydrofuran / 20 °C

With 4-methyl-morpholine; dmap; dimethylsulfide borane complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.009