2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

Base Information

Chemical Name:2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate
CAS No.:1360728-96-6
Molecular Formula:C₄H₄O₄*C₁₆H₂₅NO₃
Molecular Weight:395.453
Hs Code.:

Synonyms:2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

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Chemical Property of 2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

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Technology Process of 2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

There total 3 articles about 2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1360617-31-7
2-(3,4-dimethoxyphenyl ethoxy)-cyclohexanone

: 110-16-7,26099-09-2
maleic acid

: 1360728-96-6
2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

Guidance literature:: 2-(3,4-dimethoxyphenyl ethoxy)-cyclohexanone; With pyridoxal 5'-phosphate; isopropylamine; In dimethyl sulfoxide; at 20 - 45 ℃; pH=10.5; borate buffer;

maleic acid; In iso-butanol; at 5 - 20 ℃;

Reference yield:

: 822-87-7
2-Chlorocyclohexanone

: 1360728-96-6
2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyrrolidine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride / toluene / 4 h / 90 °C

1.2: 70 °C

2.1: isopropylamine; pyridoxal 5'-phosphate / dimethyl sulfoxide / 20 - 45 °C / pH 10.5 / borate buffer

2.2: 5 - 20 °C

With pyrrolidine; pyridoxal 5'-phosphate; isopropylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In dimethyl sulfoxide; toluene;

Reference yield:

: 7417-21-2
2-(3,4-dimethoxyphenyl)ethyl alcohol

: 1360728-96-6
2-(3,4-dimethoxyphenyl ethoxy)-cyclohexylammonium maleate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyrrolidine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride / toluene / 4 h / 90 °C

1.2: 70 °C

2.1: isopropylamine; pyridoxal 5'-phosphate / dimethyl sulfoxide / 20 - 45 °C / pH 10.5 / borate buffer

2.2: 5 - 20 °C

With pyrrolidine; pyridoxal 5'-phosphate; isopropylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In dimethyl sulfoxide; toluene;