11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Base Information

Chemical Name:11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione
CAS No.:99240-30-9
Molecular Formula:C₂₀H₂₀N₄O₅
Molecular Weight:396.403
Hs Code.:

Synonyms:11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

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Chemical Property of 11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

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Technology Process of 11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

There total 4 articles about 11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 114143-01-0
6-[(4-Ethoxy-phenyl)-furan-2-ylmethyl-amino]-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde oxime

: 99240-30-9
11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Guidance literature:: With sodium hypochlorite; triethylamine; In dichloromethane; at 0 - 10 ℃; for 3h;

Reference yield:

: 21878-48-8
N-(2-furfuryl)-p-ethoxyaniline

: 99240-30-9
11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / Et₃N / CH₂Cl₂ / 16 h

2: 60 percent / NH₂OH*HCl, NaOH / ethanol; H₂O / 12 h

3: 80 percent / 10percent aq. NaOCl, Et₃N / CH₂Cl₂ / 3 h / 0 - 10 °C

With sodium hydroxide; sodium hypochlorite; hydroxylamine hydrochloride; triethylamine; In ethanol; dichloromethane; water;

Reference yield:

: 114142-95-9
6-[(4-Ethoxy-phenyl)-furan-2-ylmethyl-amino]-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

: 99240-30-9
11-(4-Ethoxy-phenyl)-1,3-dimethyl-10,11-dihydro-1H,6aH-6,9-dioxa-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NH₂OH*HCl, NaOH / ethanol; H₂O / 12 h

2: 80 percent / 10percent aq. NaOCl, Et₃N / CH₂Cl₂ / 3 h / 0 - 10 °C

With sodium hydroxide; sodium hypochlorite; hydroxylamine hydrochloride; triethylamine; In ethanol; dichloromethane; water;