3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

Base Information

Chemical Name:3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol
CAS No.:84218-75-7
Molecular Formula:C₃₈H₄₆O₉
Molecular Weight:646.778
Hs Code.:

Synonyms:3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

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Chemical Property of 3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

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Technology Process of 3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

There total 11 articles about 3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

: 933-40-4
cycloxexanone dimethyl ketal

: 84218-74-6
3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-sn-glycerol

: 84218-75-7
3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

Guidance literature:: With toluene-4-sulfonic acid;
DOI:10.1016/S0008-6215(00)81808-X

Reference yield:

: 61236-94-0
4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl chloride

: 84218-75-7
3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 68.1 percent / tetrabutylammonium chloride, N,N-diisopropylethylamine / 1,2-dichloro-ethane / 16 h / 80 - 90 °C

2: 65.5 percent / camphorsulfonic acid / methanol / 24 h / 20 °C

3: 98.3 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 40 °C / 20 Torr

With camphor-10-sulfonic acid; tetrabutyl-ammonium chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 84218-72-4
3-O-(-4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-isopropylidene-sn-glycerol

: 84218-75-7
3-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-1,2-O-cyclohexylidene-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 65.5 percent / camphorsulfonic acid / methanol / 24 h / 20 °C

2: 98.3 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 40 °C / 20 Torr

With camphor-10-sulfonic acid; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;