6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

Base Information

Chemical Name:6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene
CAS No.:118326-95-7
Molecular Formula:C₁₅H₁₈O
Molecular Weight:214.307
Hs Code.:
UNII:S0376V3B2J
DSSTox Substance ID:DTXSID70922664
Wikidata:Q27896563

Synonyms:6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene;118326-95-7;S0376V3B2J;1,2,3,4,4a,10a-Hexahydro-6-methoxy phenanthrene, trans-;CCRIS 7435;UNII-S0376V3B2J;DTXSID70922664;6-methoxy-1,2,3,4,4a,10a-hexahydrophenanthrene;Q27896563;trans-1,2,3,4,4a,10a-hexahydro-6-methoxy phenanthrene;Phenanthrene, 1,2,3,4,4a,10a-hexahydro-6-methoxy-, trans-

Suppliers and Price of 6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

Chemical Property:

Vapor Pressure:0.00026mmHg at 25°C
Boiling Point:333.7°Cat760mmHg
Flash Point:131.9°C
Density:1.042g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:214.135765193
Heavy Atom Count:16
Complexity:271

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(C=CC3C2CCCC3)C=C1
Isomeric SMILES:COC1=CC2=C(C=C[C@H]3[C@H]2CCCC3)C=C1

Technology Process of 6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

There total 8 articles about 6-Methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4aR,10aS)-6-Methoxy-1,2,3,4,4a,9,10,10a-octahydro-phenanthren-9-ol

: 118326-95-7
6-methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 0.75h; Yield given; Heating;

Reference yield:

: 14425-76-4,101869-96-9,145474-37-9
6-methoxy-trans-1,2,3,4,4a,10a-hexahydro-9(10H)-phenanthrenone

: 118326-95-7
6-methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / aq. ethanol / 2 h / Ambient temperature

2: p-toluenesulphonic acid / benzene / 0.75 h / Heating

With sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol; benzene;

Reference yield:

: 100850-47-3
3'-methoxy-4,5-dihydro-[1,1'-biphenyl]-2(3H)-one

: 118326-95-7
6-methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene

Guidance literature:: Multi-step reaction with 7 steps

1: 20percent EtONa / ethanol

2: 39 g / p-toluenesulphonic acid / ethanol / 4 h / Heating

3: 1.) 50percent KOH, 2.) 10percent aq. HCl / 1.) H₂O, reflux, 4 h, 2.) acetone, room temp., 1 h

4: Zn/Hg, conc. HCl / toluene; H₂O / 48 h / Heating

5: ZnCl₂, acetic anhydride / acetic acid / 1.25 h / Heating

6: NaBH₄ / aq. ethanol / 2 h / Ambient temperature

7: p-toluenesulphonic acid / benzene / 0.75 h / Heating

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; sodium ethanolate; acetic anhydride; toluene-4-sulfonic acid; mercury; zinc(II) chloride; zinc; In ethanol; water; acetic acid; toluene; benzene;