2-(m-methoxyphenyl)-2-cyclohexenone oxime

Base Information

• Chemical Name: 2-(m-methoxyphenyl)-2-cyclohexenone oxime
• CAS No.: 100850-46-2
• Molecular Formula: C₁₃H₁₅NO₂
• Molecular Weight: 217.268
• Mol file: 100850-46-2.mol

Synonyms:

Chemical Property of 2-(m-methoxyphenyl)-2-cyclohexenone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(m-methoxyphenyl)-2-cyclohexenone oxime

There total 3 articles about 2-(m-methoxyphenyl)-2-cyclohexenone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3-methoxyphenyl)magnesium bromide (36282-40-3) → 2-(m-methoxyphenyl)-2-cyclohexenone oxime (100850-46-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erhitzen des Reaktionsprodukts mit Oxalsaeure und Toluol

2: aqueous HCl / Erwaermen des Reaktionsprodukts mit Pyridin

With hydrogenchloride; diethyl ether;

DOI:10.1039/jr9590001727

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 2-(m-methoxyphenyl)-2-cyclohexenone oxime (100850-46-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erhitzen des Reaktionsprodukts mit Oxalsaeure und Toluol

2: aqueous HCl / Erwaermen des Reaktionsprodukts mit Pyridin

With hydrogenchloride; diethyl ether;

DOI:10.1039/jr9590001727

Reference yield:

n-Amyl nitrite (463-04-7) + 1-Cyclohex-1-enyl-3-methoxy-benzene (1884-41-9,149902-05-6) → 2-(m-methoxyphenyl)-2-cyclohexenone oxime (100850-46-2)

Guidance literature:

With hydrogenchloride; Erwaermen des Reaktionsprodukts mit Pyridin;

DOI:10.1039/jr9590001727

upstream raw materials:

n-Amyl nitrite

1-Cyclohex-1-enyl-3-methoxy-benzene

(3-methoxyphenyl)magnesium bromide

cyclohexanone

Downstream raw materials:

3'-methoxy-4,5-dihydro-[1,1'-biphenyl]-2(3H)-one

(+/-)-[2t-(3-methoxy-phenyl)-3-oxo-cyclohex-r-yl]-acetic acid

6-methoxy-trans-1,2,3,4,4a,10a-hexahydrophenanthrene