1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol

Base Information

• Chemical Name: 1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol
• CAS No.: 1185888-44-1
• Molecular Formula: C₃₀H₃₇N₃O₅
• Molecular Weight: 519.641

Synonyms:1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol

Chemical Property of 1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol

Chemical Property:

Purity/Quality:

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Technology Process of 1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol

There total 1 articles about 1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1-O-(4,4'-dimethoxytrityl)-2-(4-bromobutoxymethyl)-2-methyl-1,3-propanediol (1185888-42-9) → 1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol (1185888-44-1)

Guidance literature:

With N,N,N′,N′-tetramethylguanidinium azide; In acetonitrile; at 20 ℃; for 5h;

DOI:10.1021/jo9014563

Reference yield:

1-O-(4,4'-dimethoxytrityl)-2-(4-azidobutoxymethyl)-2-methyl-1,3-propanediol (1185888-44-1) + 2,2'-[1,4-phenylenebis(oxy)]bisacetic acid (2245-53-6) → C40H45N3O10 (1185888-47-4)

Guidance literature:

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In pyridine; at 20 ℃; for 3h;

DOI:10.1021/jo9014563

upstream raw materials:

1-O-(4,4'-dimethoxytrityl)-2-(4-bromobutoxymethyl)-2-methyl-1,3-propanediol

Downstream raw materials:

C₄₀H₄₅N₃O₁₀

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